MAGNETIC NANOSTRUCTURES HAVE RECEIVED INCREASING INTEREST BECAUSE OF THEIR POTENTIAL APPLICATION IN MAGNETIC RECORDING MEDIA, SENSORS, AND STORAGE SYSTEMS. THEY ARE FUNDAMENTALLY IMPORTANT AS MODEL SYSTEMS TO INVESTIGATE NANOMAGNETISM WHICH IS SIGNIFICANTLY DIFFERENT FROM MAGNETIC PROPERTIES OF BULK MATERIAL. IN THE LITERATURE, THE TOP DOWN, AND THE BOTTOM UP APPROACHES ARE USED TO SYNTHESIZE LIKE NANOFLOWERS. THE MECHANOCHEMICAL SYNTHESIS IS AN INTERDISCIPLINARY NEW APPROACH BETWEEN THE TOP DOWN AND BOTTOM UP APPROACHES [1]. THE IDEA OF PERFORMING REACTIONS DIRECTLY BETWEEN SOLIDS, EXCLUDING THE DISSOLVING STAGE, IS ATTRACTIVE TO CHEMISTS BECAUSE REACTIONS IN AQUEOUS SOLUTION UNDERGO SIDE REACTIONS. THE PROPERTIES OF MAGNETIC COBALT NANOPARTICLES ARE STRONGLY DEPENDENT ON THE SIZE AND SHAPES OF METAL NANOPARTICLES. UNIFORM COLLOIDAL CO NANOPARTICLES ARE FASCINATING DUE TO THEIR OUTSTANDING MAGNETIC PROPERTIES AND VARIOUS PROMISING APPLICATIONS SUCH AS HIGH-DENSITY RECORDING MEDIA, MAGNETIC FLUIDS, DRUG DELIVERY, AND GENETHERAPY [2-3]. IN THIS PROCEDURE, COBALT LIKE NANFLOWERS WERE PREPARED FROM COBALT AZIDE COMPLEXES IN SOLID STATE BY INTRAMOLECULAR OXIDATION AND REDUCTION REACTION IN PRESENCE OF APPROPRIATE BASES. COBALT LIKE NANOFLOWERES WERE CHARACTERIZED USING XRD, SEM, VSM ANALYSES.